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1 article(s) from Rosnes, Mali H

3D-printed devices for continuous-flow organic chemistry

Vincenza Dragone,
Victor Sans,
Mali H. Rosnes,
Philip J. Kitson and
Leroy Cronin

Beilstein J. Org. Chem. 2013, 9, 951–959, doi:10.3762/bjoc.9.109

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Graphical Abstract

Figure 1: Schematic representation of the 3D-printed reactionware devices employed in this work showing the i...

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Figure 2: Flow system setup, where a R1 is connected to the syringe pumps and the ATR-IR flow cell with stand...

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Figure 3: Carbonyl compounds and primary amines used in the syntheses reported in this work. Carbonyl compoun...

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Figure 4: ATR-IR spectra of the synthesis of compounds 3b (on the left) and 3d (on the right). The spectrum o...

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Figure 5: (a) IR spectra of benzaldehyde at different concentrations. The solvent peak at 1022 cm⁻¹ remains c...

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Figure 6: Comparison of the IR spectra of imine 3a, derived from benzaldehyde (1a) and aniline (2a), synthesi...

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Figure 7: Representation of the setup for the two-step flow reaction employed in this work. The first reactor...

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Figure 8: Example of an ATR-IR graph in which an imine spectrum is compared with the reduced imine spectrum.

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Published 16 May 2013

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